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Synthesis of oxygen and nitrogen heterocycles via stabilized carbocations and ring closing metathesis. - LIST OF ABBREVIATIONS

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Synthesis of oxygen and nitrogen heterocycles via stabilized carbocations and

ring closing metathesis.

Doodeman, R.

Publication date

2002

Link to publication

Citation for published version (APA):

Doodeman, R. (2002). Synthesis of oxygen and nitrogen heterocycles via stabilized

carbocations and ring closing metathesis.

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LISTT OF ABBREVIATIONS

Ac c Anal l BF3OEt2 2 Boc c w-Bu u f-Bu u br r CSA A

cy y

d d DBU DBU DCE E DIBALH H DMAP P DMSO O DMD D DMF F d p p p p ee e Et t EtOAc c equiv v h h HRMS S IR R ƒ ƒ LDA A LHMDS S Me e Mes s min n m p p NMR R PE E Ph h t-Pr r PPTS S q q RCM M RSM M Rf Rf rt t s s t t TBS S THF F TLC C Ts s acetyl l elementall analysis borontrifluoridee etherate terf-butoxycarbonyl terf-butoxycarbonyl n-butyl l tert-buty\ tert-buty\ broadd (spectral) camphorsulfonicc acid cyclohexyl l

day(s);; doublet (in NMR)

l,8-diazabicyclo[5.4.0]undec-7-ene e 1,2-dichloroethane e diisobutylaluminiumm hydride 4-(dimethylamino)pyridine e dimethylsulfoxide e dimethyldioxirane e N,N, N-dimethy Iformamide bis(diphenylphosphino)propane e enantiomericc excess ethyl l ethyll acetate equivalent t hour(s) )

highh resolution mass spectrum infrared d

couplingg constant (in NMR) lithiumm diisopropylamide lithiumm hexamethyldisilazide methyl l

2,4,6-trimethylphenyl l minute(s) )

meltingg point (range) nuclearr magnetic resonance petroleumm ether (60-80) phenyl l isopropyl l pyridiniumm para-toluenesulfonate quartett (in NMR) ring-closingg metathesis ringsluitingsmetathese e

retentionn factor (in chromatography) roomm temperature

singlett (in NMR) triplett (in NMR)

fert-butyldimethylsilyl fert-butyldimethylsilyl tetrahydrofuran n

thinn layer chromatography para-toluenesulfonyl l

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